Data File D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.DSample Name: CPK2015-114-07405=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 76Acq. Instrument : HY-LCMS-02 Location : Vial 64Injection Date : 1/14/2015 6:29:56 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\100-1000MS+3MIN. MLast changed : 1/14/2015 5:23:36 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_4C-H01RS(RP-HPLC).MLast changed : 1/15/2015 9:59:30 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13024 Batch#07405 A-RP-32 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.D) 1.707 1.816mAU1000800600400 1.392 1.558 1.99320000.51 2.5151.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.392 MM 0.0552 7.76967 2.34440 0.2092 2 1.558 MM 0.0476 3.77900 1.32384 0.1017 3 1.707 MF 0.0489 3689.73657 1257.60437 99.3315 4 1.816 FM 0.0321 10.24253 5.31738 0.2757 5 1.993 MM 0.0485 1.56278 5.36536e-1 0.0421 6 2.515 MM 0.0662 1.47909 3.72632e-1 0.0398 Totals : 3714.56964 1267.49915 ===================================================================== *** End of Report ***HY-LCMS-02 1/15/2015 9:59:32 AM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.DSample Name: CPK2015-114-07405=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 76Acq. Instrument : HY-LCMS-02 Location : Vial 64Injection Date : 1/14/2015 6:29:56 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\100-1000MS+3MIN. MLast changed : 1/14/2015 5:23:36 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_4C-H01RS(RP-HPLC).MLast changed : 1/15/2015 10:01:03 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13024 Batch#07405 A-RP-32 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.D) ES-API, Pos, Sc 1.69222500020000017500015000012500010000075000500002500000.511.522.53min HY-LCMS-02 1/15/2015 10:01:04 AM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.DSample Name: CPK2015-114-07405MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.692 949540 555.20 I 554.20 I 277.70 I*MSD1 SPC, time=1.671:1.707 of D:\\AGLIENT 1260\\DATA\\20150114\\20150114 2015-01-14 10-44-04\\CPK2015-114-07405.D ES-API 277.7100806040200100200Max: 72936 556.2 555.2 554.2300400500m/z *** End of Report ***HY-LCMS-02 1/15/2015 10:01:04 AM Li Shan(LCMS-02)Page 2 of 2