MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\CPK\\CPK2016-N10-11138.D Tgt Mass (EZX): 560.00 Injection Date : 10 Nov 16 1:12 pm +0800 Seq. Line : 0 Sample Name : CPK2016-N10-11138 Location : P1-F-04 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-13311 Batch#11138 Easy-Access Method: '1-POS-3MIN' 560.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C *DAD1 B, Sig=214,4 Ref=off mAU1500100050000.5*DAD1 C, Sig=254,4 Ref=off mAU80060040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7030000020000010000000.511.5 Ion 561, MSD1 561,Target Mass 560 +H Positive, EIC=560.7:561.7 1500010000500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.34522.5min1.34311.3481.2951.3481.522.5min*1.6051.522.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.02 2.41 1.78 0.12 281 1.35 0.02 2002.86 2101.68 99.88 281 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.35 0.02 945.74 1007.17 99.87 281 1.60 0.02 1.21 0.00 0.13 233HY-LCMS-02 11/10/2016 13:17:33 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.34 <<<< POSITIVE SPECTRA >>>> ES-API Positive300002500020000 560.3 157.3 563.2150001000050000200300400500600700800900m/z 280.7 281.6HY-LCMS-02 11/10/2016 13:17:33 KFF(LCMS-02)Page 2 of 2